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The NMR Spectroscopy Facility

Solid?phase Reaction Monitoring

The HR-MAS NMR probe allows reaction monitoring by NMR spectroscopy without removing the substrate from the support. The illustrated series of reactions utilised in the preparation of a solid-supported protected alanine residue were followed on resin.

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Data Collection

Bruker DPX400/2 FT-NMR spectrometer (legacy)

4 mm HR-MAS probe

Reaction scheme. N. J. Wells, PhD Thesis, University of Southampton, 2002.
Proton HR-MAS spectra. N. J. Wells, PhD Thesis, University of Southampton, 2002.
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