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The University of Southampton
The NMR Spectroscopy Facility Capabilities

5?[(benzyloxy)methyl]?3,3,4,4?tetrafluorotetrahydrofuran?2?ol

5–[(benzyloxy)methyl]–3,3,4,4–tetra

5-[(benzyloxy)methyl]-3,3,4,4-tetrafluorotetrahydrofuran-2-ol is a fluorinated monosaccharide.

A. J. Boydell, V. Vinader and B. Linclau, Angew. Chem. Int. Ed . 2004 , 43 , 5677 - 5679; Angew. Chem . 2004, 116 , 5795 - 5797.

Data Collection

Bruker DPX400/2 FT-NMR spectrometer (legacy)

5 mm SEF probe

1D fluorine NMR spectra. Top: 19F NMR spectrum; Lower: 19F{1H} NMR spectrum
FF COSY. The FF COSY spectrum shows the fluorine couplings within the molecule.
In the HF correlation spectrum the couplings between proton and fluorine can be observed as cross-peaks
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