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Southampton Chemistry Analytical Solutions

Multinuclear (Broadband) NMR Spectroscopy

The anion [NbF 6 ] -

Example spectra:

(a) 93 Nb NMR spectrum showing a binomial septet from coupling to the six 19 F nuclei (I = 1/2, 100% natural abundance, 1 J Nb-F = 335 Hz).

(b) 19 F NMR spectrum showing 10 lines from coupling to the 93 Nb nucleus (I = 9/2, 100% natural abundance, 1 J Nb-F = 335 Hz).

(a) Niobium NMR spectrum
(b) Fluorine NMR spectrum

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M. Jura, W. Levason, G. Reid and M. Webster, Dalton Trans. 2009, 7610. M. Jura, W. Levason, R. Ratnani, G. Reid and M. Webster, Dalton Trans. 2010, 883

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