All submitted samples must be accompanied by a 1 H spectrum recorded on one of the open-access spectrometers.
NMR tubes MUST be at least 19 cm long, unchipped and with a tight-fitting cap.
Seal the top of tubes containing unpleasant or toxic samples with Parafilm.
For low sample quantities in hygroscopic solvents (e. g. d6-DMSO, D2O):
Important:
Variable temperature (VT) NMR experiments | Consider the properties of the solvent (e.g. freezing or boiling point). |
Heteronuclear NMR experiments | Indicate the anticipated chemical shift and the literature reference signal. |
It is the responsibility of the submitter to find this information.
Leave samples in tray in the open access 400 room (27:1021).