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The University of Southampton
Southampton Chemistry Analytical Solutions

High?Resolution MAS NMR Spectroscopy

The HR-MAS NMR probe can be used to follow reactions on solid supports.

The following series of reactions in the preparation of a solid-supported protected alanine residue were examined by NMR spectroscopy using a 4 mm HR-MAS probe.

Reaction scheme
Proton HR-MAS NMR spectra

N. J. Wells, PhD Thesis, University of Southampton, 2002.


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